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S.W. Kim 1 Article
A Study of Electro-Discharge-Sintering of Ti-6Al-4V Spherical Powders Doped with Hydroxyapatite by Spex Milling and Its Consolidation Characteristics
Y.J. Cho, Y.H. Kim, Y.H. Jo, M.J. Kim, H.S. Kim, S.W. Kim, J.H. Park, W.H. Lee
J Powder Mater. 2013;20(5):376-381.
DOI: https://doi.org/10.4150/KPMI.2013.20.5.376
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Spherical Ti-6Al-4V powders in the size range of 250 and 300 µm were uniformly doped with nano-sized hydroxyapatite (HAp) powders by Spex milling process. A single pulse of 0.75-2.0 kJ/0.7 g of the Ti-6Al-4V powders doped with HAp from 300 mF capacitor was applied to produce fully porous and porous-surfaced Ti-6Al-4V implant compact by electro-discharge-sintering (EDS). The solid core was automatically formed in the center of the compact after discharge and porous layer consisted of particles connected in three dimensions by necks. The solid core increased with an increase in input energy. The compressive yield strength was in a range of 41 to 215 MPa and significantly depended on input energy. X-ray photoelectron spectroscopy and energy dispersive x-ray spectrometer were used to investigate the surface characteristics of the Ti-6Al-4V compact. Ti and O were the main constituents, with smaller amount of Ca and P. It was thus concluded that the porous-surfaced Ti-6Al-4V implant compacts doped with HAp can be efficiently produced by manipulating the milling and electro-discharge-sintering processes.

Citations

Citations to this article as recorded by  
  • Effect of heat treatment on the microstructural and mechanical properties of Ti6Al4V-equine bone nanocomposites
    Wonki Jeong, Se-Eun Shin, Hansol Son, Hyunjoo Choi
    Materials Characterization.2021; 179: 111361.     CrossRef

Journal of Powder Materials : Journal of Powder Materials